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-The Project Gutenberg EBook of The Dry Collodion Process, by Charles Long
-
-This eBook is for the use of anyone anywhere in the United States and most
-other parts of the world at no cost and with almost no restrictions
-whatsoever. You may copy it, give it away or re-use it under the terms of
-the Project Gutenberg License included with this eBook or online at
-www.gutenberg.org. If you are not located in the United States, you'll have
-to check the laws of the country where you are located before using this ebook.
-
-Title: The Dry Collodion Process
-
-Author: Charles Long
-
-Release Date: November 20, 2020 [EBook #63814]
-
-Language: English
-
-Character set encoding: UTF-8
-
-*** START OF THIS PROJECT GUTENBERG EBOOK THE DRY COLLODION PROCESS ***
-
-
-
-
-Produced by Tom Cosmas from images kindly made available
-from The Internet Archive. All materials are placed in the
-Public Domain.
-
-
-
-
-
-
-
-
-Transcriber Note
-
-Text emphasis is denoted as _Italics_ and =Bold=.
-
-
-
-
- THE DRY COLLODION PROCESS.
-
-
- BY
-
- CHARLES A. LONG.
-
-
- THIRD EDITION.
-
- PUBLISHED BY BLAND & LONG, OPTICIANS,
-
- AND
-
- PHOTOGRAPHIC INSTRUMENT MAKERS TO HER MAJESTY,
-
- [Illustration]
-
- BY APPOINTMENT.
-
- 153, FLEET STREET, LONDON.
-
-
- ENTERED AT STATIONERS' HALL,
-
- _Price 1s. Per Post 1s. 1d._
-
- 1858.
-
-
- H. SILVERLOCK, PRINTER,
- WARDROBE TERRACE, DOCTORS' COMMONS, LONDON, E.C.
-
-
-
-
-
-PREFACE TO FIRST EDITION.
-
-
-The following pages shall be devoted to the description of
-a process on Dry Collodion, which I believe to be at once simple and
-effective. The experiments connected with the perfection of this
-process have occupied my leisure time for the space of two years
-or more, and have been conducted with all the care of which I was
-master. The constant repetition of them enables me to say, that
-whoever will follow diligently the process step by step, as detailed
-in this Pamphlet, must succeed in producing pictures in every way
-such as could be required by the most exacting critic.
-
-The process is simple, clean, and expeditious; and the resulting
-Negatives possess the exquisite softness of Albumen, the brilliancy
-of the wet Collodion, and the fine artistic texture of the Paper
-process.
-
-To disarm criticism, and to make peace with my fellow labourers in
-the art, I wish it to be understood that I do not claim the use of
-Collodion, of Gelatine, of Metagelatine, or of any of the Chemicals
-used in the process--most of these have been employed by others in
-various ways; I merely reserve to myself the pleasure of placing
-in the hands of Photographers a definite and simple plan by which
-pictures may be taken on Dry Collodion.
-
- CHARLES A. LONG.
-
- _June 20, 1857._
-
-
-
-
-PREFACE TO SECOND EDITION.
-
-
-In issuing a second edition of the Dry Collodion process,
-I would take occasion to remark, that after some months' practical
-working, it has not been found necessary to make any material
-alteration in the process; success has usually attended the adoption
-of it, and in those cases where good pictures have not resulted, the
-failure has always been traced to the use of a Collodion not suited
-to the process.
-
-I cannot allow this opportunity to pass, without thanking those
-gentlemen whose opinions possess weight in matters photographic, for
-the very candid manner in which they have tested the capabilities of
-my process, and for the very flattering testimony they have borne to
-its efficiency, simplicity, and certainty.
-
- CHARLES A. LONG.
-
- 153, Fleet Street,
-
- _September 1857_.
-
-
-
-
-PREFACE TO THIRD EDITION.
-
-
-The process described in the following pages has now been
-in use for twelve months, and I have much satisfaction in stating
-that it has, in almost every instance where it has been adopted and
-carried out with care and attention, yielded results which leave
-scarcely anything to be desired.
-
-The present Edition might more properly be termed a reprint, as the
-alterations in the text do not extend to more than a few matters of
-detail, which experience has shewn to be desirable, the principles of
-the process remaining undisturbed.
-
- CHARLES A. LONG.
-
- 153, Fleet Street,
-
- _June 1858_.
-
-
-
-
-OPINIONS OF THE PRESS.
-
-
-_From the Athenæum._
-
-We have not merely examined the description given by Mr. Long of his
-dry collodion process, but we have witnessed the results obtained by
-following carefully his directions. It appears to us that, by it, a
-collodion plate may be prepared at home, wrapped in paper, and packed
-in portmanteau; that we may journey to Rome or Venice, then place
-our plate in the camera obscura, and allow it for a few minutes to
-receive the luminous image; remove it in a dark room; re-pack it
-and trouble ourselves no more about it until our return to England;
-when, in the room in which it was prepared, we may witness the magic
-process of development, and rejoice that we have, without much
-labour, secured a picture of the Coliseum or of the Bridge of Sighs.
-
-
-_From the Journal of the Cambrian Archæological Association._
-
-New Photographic Process.--Mr. Long, of the firm of
-Bland and Long, Opticians, Fleet Street, has recently put forth a
-valuable pamphlet, in the form of an essay on the dry collodion
-process. By means of this, plates prepared weeks beforehand may
-be exposed to objects, and then kept for weeks afterwards before
-they are developed, as he has proved it himself on the Continent.
-The advantage of this process to travellers, and especially to
-archæologists, is immense; because hitherto the main drawback upon
-photography has been the trouble and expense of carrying chemicals,
-tents, &c. &c., besides the camera, with its lenses, to the scene of
-operation. Now, however, it will be sufficient to carry merely the
-camera, with a suitable supply of plates prepared according to this
-process. The observer can then, by merely exposing his plates, with
-the proper precautions, _bag_ any number of views per diem, and on
-his return home can develop them--or have them developed--at leisure.
-If this process succeeds, it will have the effect of splitting
-photography into two distinct branches--the _æsthetic_, and the
-_practical_. The former will fall to the share of the intelligent
-observer, the traveller, the man of taste, who will go and search
-for objects, combine them, or use them, under the most favourable
-æsthetic circumstances, and then will carry them home to be handed
-over to the man of practice. Once in his hands, nothing will remain
-but to manipulate the plates according to the rules of photographic
-science, by means of all the best appliances that a well fitted
-laboratory can furnish. One branch will feed the other. One will be
-the department of observation, of search, of taste, of beauty; the
-other will be that of calm scientific development, of improvement,
-of preservation. One man will be like the artist who paints; the
-other like the artist who engraves. One will be like the author, the
-man who writes; the other like the printer, the man who perpetuates.
-We recommend members to enquire carefully about this new process;
-because if it becomes firmly established, any archæologist moving
-about the Country may get views of churches, castles, cromlechs,
-meini-hirion, seals, &c. &c., _usque ad satietatum_--we had almost
-said _ad nauseam_; but that word can never be connected with
-archæology! The upshot of this is,--"Read Mr. Long's pamphlet, and
-set up a portable camera with his prepared plates, as we intend doing
-ourselves!"
-
-
-_From the Liverpool and Manchester Photographic Journal._
-
-We must advise all who are interested in dry processes to obtain Mr.
-Long's clearly written pamphlet. (Leader, July 15th, 1857.)
-
-
-_Extract from Proceedings of Charlton Photographic Society, October
-8th, 1857. Paper by Mr. Hooper,--On the results of his experience in
-the practice of several Preservative Processes._
-
-I commenced experimenting on the process of Mr. Long. The success I
-have met with from the first has convinced me that that process will
-ere long be generally adopted: the plates being easily and quickly
-prepared, and keeping well, is a great advantage.
-
-
-_Extract from Letter from G. R. Smith, Esq., to the Editor of the
-London Photographic Journal, Sept 21, 1857._
-
-My tour of a fortnight's duration having ended, I returned to London,
-and began developing (the dry plates). To my great delight, I found
-all Mr. Long had said in favour of his process fully realized.
-Picture after picture (I took twenty-eight) came out with great
-beauty, and so far as the process is concerned, I have not had a
-single failure.
-
-
-_Mr. Long's Dry Collodion Process._
-
-_Letter from Robert Hunt, Esq., F.R.S., to the Editor of the London
-Photographic Journal, October, 1857._
-
- 6, Green's Row, Chelsea.
-
-Sir,--It is due to Mr. Long that I should state what my experience
-has been with his dry collodion plates, and I feel much satisfaction
-in doing so, being enabled fully to confirm all that Mr. Smith has
-said respecting the dry plates prepared as he has described (Photo.
-Journ. Sept. 21). On the 26th of August, Mr. Long, at my request,
-furnished me with some of his dry collodion plates. Absence from
-London, and the press of official engagements, prevented my trying
-any experiments with those plates until the 30th of September.
-Although the weather was very unfavourable, the result was superior
-to my expectations. On the 7th of October, at four in the afternoon,
-when the sky was covered with clouds and the weather stormy, I
-exposed a plate in the camera obscura for ten minutes to the dark
-brick building, Chelsea Hospital. I enclose you a positive print from
-the result of this experiment. When we remember that the sensitive
-plate had been kept by me for a period of _forty-two days_, and then
-exposed under very unfavourable circumstances, I think you will admit
-that the result is satisfactory. I should not content myself with
-this trial, but that I am again compelled to leave London for a long
-period, and I shall have no other opportunity of testing these plates
-for this year. I feel convinced that the traveller might with perfect
-safety use plates which have been prepared for a month, and thus
-relieve himself from much labour and frequent annoyance, by the use
-of Mr. Long's process.
-
- Robert Hunt.
-
-
-_From the Illustrated London News, January 9, 1858._
-
-It is but a few years since, when we heard with surprise, and
-some incredulity, that light could be made to delineate images of
-external objects upon chemically prepared tablets placed in the
-camera obscura,--now photography stares us in the face at every
-corner,--that which was wonderful has become familiar,--that which
-was mysterious is singularly common.
-
-In cities, we see glass houses, on at least one roof in every
-street,--in villages, caravans, with Brown and Jones, photographers,
-are regularly found,--on the hills we discover the tent, and in the
-valleys the camera,--by the river-side there is the mysterious head
-hidden in the dark curtains of a dark box,--and upon the sea-shore
-the tripod-stand is securely fixed in the sands, and a biped is
-evidently focusing for the next fine ocean wave,--the sketcher has
-fled to his own especial solitudes, and the photographer has usurped
-his place.
-
-It has been said of the most recent photographic processes, as was
-well said of the octo-syllabic verse, that it possesses "unfortunate
-facilities." This is true in many respects of the positive collodion
-process, by which the myriads of sad reflections on humanity are
-perpetrated. Not so, however, is it with the negative process, by
-which alone we can multiply the beautiful things which the solar
-pencil traces with such fidelity. The labour attendant upon a
-photographic tour is great, and real enthusiasm alone carries the
-amateur forward. The camera obscura and the stand are a burden, and
-with the tent and chemical box, they become a real load. Then there
-is the uncertainty attendant upon the processes. We deal with the
-nicest chemical adjustments. The balance is arranged with caution for
-a certain set of conditions,--alter but one of these, and all goes
-wrong. We leave home in the morning, we work in the dark all day, and
-we return jaded at night, to find we have obtained--nothing.
-
-Sensitive as the collodion process is, and charming as are the
-results, when all goes on successfully, it has not hitherto been
-a process which can be practised out of doors, without many
-extraordinary, expensive, and troublesome appliances.
-
-It is, therefore, with very much satisfaction that we have watched
-the progress of the so-called "dry collodion processes." Nearly
-all the processes that have been published,--the "gelatine,"--the
-"oxymel,"--the "glycerine," and others,--have much that is excellent
-in them; but it appears to us that a dry collodion process devised by
-Mr. Long, of which he has recently published a description, is more
-simple and effective than any other. We have seen beautiful pictures
-obtained in Belgium upon plates prepared in England, and which plates
-were brought to this country again before the pictures were developed.
-
-Any man may, previously to starting on his journey, prepare, or
-purchase prepared, a stock of glass plates. Armed with these and his
-camera, he may proceed to
-
- "Where the bleak Swiss their stormy mansion tread.
- And force a churlish soil for scanty bread;"
-
-or to that
-
- "------sea Cybele fresh from ocean
- Rising with her tiara of proud towers,"--
-
-and, resting on his way, he may adjust his camera and his plate, and
-in the few minutes which, under any circumstances, he would spend in
-observation, he secures a picture for future study,--a photograph to
-give him pleasure in the quiet of his home.
-
-Mr. Long has published a little treatise, with which we head this
-article, and by following out the simple directions which he gives,
-all may succeed in obtaining the important desideratum,--a parcel
-of highly sensitive plates, which can be packed in paper and stowed
-away in a portmanteau, to be drawn out as occasion may require, to
-be returned again to the same package (without having any of the
-annoyances attendant upon a box of liquid chemicals), and a plate
-which can be kept with its dormant picture quite uninjured until the
-photographer, on his arrival home, at his perfect leisure, in his own
-operating room, can develop the photograph which he has obtained.
-
-Such are the facilities offered by this improvement, that we may
-expect almost every traveller will avail himself of it, and thus
-secure for his own portfolio, and the portfolios of his friends,
-views of scenes hallowed by their historical association,--of ruins
-rendered sacred from the sacred memories which still wrap them in
-their shadows, as the mantling ivy clothes their crumbling walls.
-
-
-
-
- THE
-
- =DRY COLLODION PROCESS.=
-
-
-Before describing in detail the manipulations of the process
-on Dry Collodion plates, it will be necessary to say a few words
-on the materials and apparatus to be employed, and also to give an
-account of the means of preparing the various solutions used in the
-process. First,
-
-
-THE COLLODION.
-
-This being the principal material we have to use, we must exercise
-great care in the selection of a sample that possesses all the
-characteristics which fit it for a dry process. We must reject all
-samples that possess great tenacity and contractile power: the
-Collodion must not be too thick, and it must flow evenly over the
-plate, and not set in ridges. The best condition for the Iodized
-Collodion is that known as _powdery_, that is, being spread on the
-plate and partially dry, it cannot be removed as a film, but crumbles
-up on being pressed by the finger in its passage across the plate; in
-fact, such a condition as would arise from using gun cotton prepared
-with acids at a high temperature.
-
-The following formula will be found to answer most admirably:
-
- Gun Cotton 60 grains.
- Absolute Alcohol 5 ounces.
- Sulphuric Æther, sp. gr. ·730 15 ounces.
-
-The cotton is to be shaken up with the mixture of alcohol and æther,
-and when dissolved, the bottle containing it must be stood aside, in
-order that any undissolved particles of cotton may subside. The clear
-liquid may then be decanted into a clean bottle for use.
-
-It will be as well to test the quality of the Collodion thus prepared
-before coating any number of plates with it, for, although the above
-proportions are very excellent, some little latitude must be allowed
-for the different degrees of solubility of the various samples of
-cotton used from time to time. The film, when spread, on the glass
-plate and partially dry, should not be capable of being removed in
-the form of a skin, but should give before the finger and crumble up
-on its being rubbed across the plate.
-
-Should any difficulty, however, occur, it would be better to obtain
-a sample of the Collodion made by an experienced hand, in order that
-a fair trial may be given to the process. If the Collodion be too
-contractile it will give rise to blisters in the film, and will wash
-off the plate during development.
-
-The Iodizing Solution that I have found to give the best
-results in this process is made in the manner following:--
-
- Absolute Alcohol 8 ounces.
- Iodide of Cadmium 64 grains.
- Iodide of Ammonium 64 grains.
-
-The iodides are to be dissolved by agitation in the alcohol, and the
-resulting solution is to be carefully filtered, and preserved in a
-well stoppered bottle.
-
-The Iodized Collodion consists of--
-
- Iodizing Solution 2 drams }
- } 1 ounce
- Plain Collodion 6 drams }
-
-The Collodion should always be iodized at least twelve hours before
-it is required; this interval allows any insoluble matters either
-from the iodizing solution or from the Collodion itself to fall to
-the bottom, and enables the operator to pour off the clear solution
-into a perfectly clean bottle for use.
-
-Next in importance to the Iodized Collodion comes
-
-
-THE PRESERVATIVE SOLUTION.
-
-Some care is required in the preparation of this solution, in order
-that it may be clear and bright when finished, and not contain
-particles that would be deposited in its passage over the Collodion
-film when being used. The chief precaution to be observed is _not to
-allow it to boil too rapidly, and not to conduct the operation over
-too fierce a fire;_ attention to this will prevent many failures,
-and ensure a solution in every way suited for the process.
-
-Take one ounce of the best transparent gelatine, and throw it into
-a pipkin in which has been previously placed one pint of distilled
-water; set this on a slow fire, or over a lamp, until the gelatine
-is completely melted; then weigh out half ounce of pure citric acid
-and dissolve it in two ounces of distilled water; add this to the
-solution of gelatine, stirring it during the addition with a glass
-rod. The solution in the pipkin is now to be gently boiled for about
-half an hour: remove it from the fire, and add sufficient distilled
-water to make up the bulk of liquid to one pint. When quite cold, the
-liquid in the pipkin is to be filtered through two thicknesses of
-pure white blotting paper into a bottle perfectly dry and clean. We
-now add to every pint of filtered preservative solution, two ounces
-of alcohol of the specific gravity of ·840.
-
-The solution thus prepared is ready for use, and should be of a pale
-amber colour, without any signs of insoluble particles floating in
-it; should any appear after it has been prepared for some days, a
-second filtration will remove them, and render the liquid again
-bright and clear.
-
-It will be found better to prepare this solution only in the quantity
-indicated above, unless the consumption be large, for, although it
-will keep good for a month or more, my experience points to the fact,
-that the most successful results follow the use of Preservative
-Solution freshly prepared.
-
-
-THE NITRATE OF SILVER BATH.
-
-The bath for rendering the plates sensitive does not differ from that
-recommended for taking negatives with wet Collodion. The formula for
-its preparation may not be out of place, however, and may assist
-those whose knowledge of the matter is not perfect.
-
- Nitrate of Silver (fused) 1¼ ounces.
- Distilled Water 1 pint.
- Iodide of Cadmium 3 grains.
-
-Dissolve the nitrate of silver in half the water and then add the
-iodide of cadmium; thoroughly agitate the mixture for five or ten
-minutes, then add ½ ounce of alcohol, sp. gr. ·840, and fill up
-with the remaining half of the distilled water; further agitation,
-and subsequent filtration through two thicknesses of white bibulous
-paper, will put us in possession of a negative bath. The nitrate of
-silver being fused, and consequently, pure and neutral, and as it is
-essential to obtain clean pictures that the bath should be slightly
-acid in its reaction, we find it necessary to add 5 or 6 minims or
-drops of pure glacial acetic acid to a bath of 20 ounces, in order
-that the above condition may obtain.
-
-
-THE DEVELOPING SOLUTION
-
-Is very simple in its nature, being merely a saturated solution
-of gallic acid in distilled water, to which has been added a small
-proportion of alcohol of sp. gr. ·840.
-
-The exact formula is as follows:--
-
- Distilled Water 1 pint.
- Alcohol sp. gr. ·840 1 ounce.
- Gallic Acid ½ ounce.
-
-The gallic acid will not be entirely dissolved, but that left at the
-bottom of the bottle will ensure the solution being saturated; it is
-better not to filter the developing solution until it is required
-for use, as it is preferable to allow it to stand over an excess of
-gallic acid, than for it to be withdrawn after a slight agitation
-with the crystals; it is a great error to suppose that we obtain a
-saturated solution of gallic acid by merely agitating the crystals
-with water for a few moments.
-
-The developing solution prepared as above directed will keep good and
-in working order for some weeks, but when it becomes of a dark color,
-it would be safer to reject it and prepare a fresh quantity than to
-run the risk of a failure from an impure and imperfect developing
-agent.
-
-
-NITRATE OF SILVER SOLUTION,
-
-For adding to the gallic acid during development, is composed of
-
- Fused Nitrate of Silver 30 grains.
- Distilled Water 1 ounce.
-
-
-THE FIXING SOLUTION
-
-Consists of a solution of hyposulphite of soda in water, (filtered,)
-in the following proportion:--
-
- Hyposulphite of Soda in crystals 8 ounces.
- Rain or Filtered Water 1 pint.
-
-The Apparatus, &c. required in the Dry Collodion process is
-of the most simple kind, and consist of the following items
-
- Glass plates.
- Pneumatic plate holders.
- Plate holder, for cleaning the plates.
- Glass or porcelain dishes.
- Glass or gutta percha dipping bath and dipper.
- Silver hook, for lifting plates.
- Levelling stand.
- Measures, 1, 2, and 4 ounce.
- Glass funnels.
- Wash leather.
- Some clean cloths and broad camel's hair brush.
- Cotton wool.
- Bibulous paper.
- [A] The Chemicals are--
- Nitrate of silver (fused.)
- Glacial acetic acid.
- Iodized Collodion (dry.)
- Gelatine.
- Citric Acid.
- Alcohol.
- Sulphuric æther.
- Gallic acid.
- Hyposulphite of soda.
- Iodide of cadmium.
- Benzoin varnish.
-
-[A] The dry Collodion and the various solutions, ready for use, may
-be obtained of the Publishers.
-
-In the above List we presume that the operator is in possession of a
-suitable camera and lens, and the usual adjuncts of camera tripod,
-&c. &c. These should all be of the best kind, otherwise it will be
-impossible to obtain good results.
-
-[Illustration]
-
-
-=THE MANIPULATION.=
-
-The process of obtaining a picture on Dry Collodion plates is in
-itself a most simple and easy matter, but there are one or two
-precautions that appear necessary to ensure success that cannot be
-lightly neglected. In the first place, it is absolutely certain,
-that if we want a clean and bright picture, we must have a plate
-perfectly free from all extraneous matters, such as soap, grease,
-&c. Various plans for cleaning the glass plate have been proposed,
-all more or less successful, but in most of them there is one great
-fault, namely, that of using a powder, as tripoli, rotten-stone,
-&c. to rub off the dirt with. Now we find that in practice this
-will not answer, from the almost impossibility of getting rid of
-the floating particles of the powder when the plate is rendered
-slightly electrical by rubbing, and as each of these particles if
-it become enveloped in the Collodion film, would produce a spot on
-the finished picture, we find it necessary to search in another
-direction for a detergent for the glass plate to which this objection
-would not apply. One soon presents itself in the form of _old waste
-Collodion_--this spread on the glass plate and rubbed off again
-with cotton wool, makes the best and most perfect cleanser hitherto
-proposed, without any of the objections usually appended to other
-materials used for the same purpose.
-
-The next precaution necessary to be observed is, that all the
-solutions should be perfectly bright and clear; they should be
-absolutely free from floating particles of any kind. This is
-essential, as it is impossible to obtain clean pictures without
-attention to it; the floating bodies in the solution settle on the
-plate, and form so many nuclei, around which, in the development of
-the picture, the silver is deposited in an opaque mass, forming spots
-and blemishes on the surface of the plate.
-
-There is one precaution that cannot be dispensed with, and that
-is, to be sure that the chemicals employed are of absolute purity;
-without this, success is very problematical, and vexation and disgust
-the sure reward of its neglect.
-
-The process may for convenience be divided into the following
-stages:--
-
- 1.--Cleaning the plate.
- 2.--Coating it with Collodion.
- 3.--Rendering the plate sensitive.
- 4.--Applying the Preservative solution.
- 5.--Exposure in the camera.
- 6.--Development of the picture.
- 7.--Fixing the developed image.
- 8.--Varnishing the finished negative.
-
-CLEANING THE PLATE.
-
-[Illustration: _Fig. 1._]
-
-The glass plate is first to be thoroughly washed with an abundance
-of water, and dried on clean cloths; it is then to be placed in the
-plate holder (_Fig. 1_), and have poured over its upper side a
-small quantity of old Collodion. Now take a tuft of cotton wool and
-rub the Collodion all over the plate, giving the hand a circular
-motion at the time: keep rubbing until the Collodion is very nearly
-dry, then turn the plate in the holder and repeat the same treatment
-with the opposite side; then lean the plate thus treated against a
-wall, while another, or any number are put through this stage. When
-a sufficient number have been so far cleaned, the plate holder is
-to be carefully wiped, and the first plate--the edges of which have
-also been carefully wiped with a _clean_ cloth--is to be replaced,
-and treated with a smart rubbing with a wash leather, the operator
-at intervals gently breathing on the plate. Both sides of the plate
-being cleaned in this way, it may be removed, after again wiping the
-edges carefully, to the plate box, to await the subsequent steps of
-the process. Plates cleaned in this manner should look perfectly
-transparent, and free from any marks of the cloth or leather, and
-when breathed upon should condense the moisture of the breath in
-one uniform degree over the whole surface. If patches of uneven
-condensation appear, a repetition of the process must be had recourse
-to.
-
-The plate being clean, we proceed to the next step,
-
-
-COATING THE PLATE.
-
-Lay a piece of clean blotting paper on the table, larger than the
-plate we are about to use; place the clean plate on this, and
-then bring the pneumatic plate holder to bear on the centre of the
-glass, making sure that it has laid hold firmly. We then raise the
-plate with the left hand, and bring the surface upwards which was
-previously on the blotting paper; it will no doubt be found that
-small particles of dust have attached themselves to the plate, these
-must be removed by a broad and soft camel's hair brush, kept for this
-purpose only.
-
-[Illustration: _Fig. 2._]
-
-The Collodion is then to be poured on, as shown in the diagram (_Fig.
-2_), and the superfluous quantity returned to the bottle from one of
-the corners of the plate. It does not matter which of the corners is
-used for this purpose, that which is most convenient to the operator
-assuming the preference. If the Collodion should have a tendency to
-set in ridges across the plate, a rocking motion, while the delivery
-corner is in the mouth of the bottle, may be given to it, still
-keeping the plate in a vertical plane. This will restore the film to
-perfect evenness and freedom from irregularity of any sort. The plate
-should be held in the vertical position for a few moments before
-being placed on the dipper to undergo the next operation of
-
-
-RENDERING THE PLATE SENSITIVE.
-
-[Illustration: _Fig. 3._]
-
-The plate being placed, coated side outwards, on the dipper, is to
-be plunged without hesitation into the nitrate of silver bath (_Fig.
-3_). This must be done without stopping, otherwise a line across the
-plate will indicate, on development, the position of the plate in
-the bath at the time this stoppage took place; so that if we were to
-immerse the plate by a series of jerks, we should have as a result,
-so many bands of unequal development in the finished picture; showing
-the importance of plunging the plate into the bath without any
-stoppage during its descent.
-
-[Illustration: _Fig. 4._]
-
-When the plate has rested for half a minute in the bath, it may be
-withdrawn, and quickly re-immersed. This washing must be continued
-at intervals, until the greasy appearance goes off, generally for
-the space of two minutes, when the plate is to be taken out of the
-bath and placed with its lower edge on a pad of blotting paper, in a
-position as shown in the cut (_Fig. 4._) A fragment of blotting paper
-is then to be used to absorb the moisture from the back of the plate,
-and a pneumatic plate holder--which should only be used for this
-purpose--is applied to it to form a support while
-
-
-APPLYING THE PRESERVATIVE SOLUTION.
-
-[Illustration: _Fig. 5._]
-
-Taking the plate in the left hand by means of the pneumatic holder,
-incline it as shown in the diagram (_Fig. 5_); then having poured
-into a perfectly clean measure rather more of the preservative
-solution than is necessary to cover the plate twice,[B] pour half of
-it along the upper edge (A B) in such a manner, that a wave of the
-solution may flow uniformly from one end of the plate to the other;
-allow this to flow off into the waste pan or sink, and then bring the
-plate to the horizontal position, and pour on the remainder of the
-preservative solution, eight times at least, allowing it to flow
-back into the measure from each corner in succession, in order that
-the whole plate may be brought uniformly under its influence. The
-plate is to be again placed on a piece of clean blotting paper (as
-shown at _Fig. 4_), and its back once more wiped with a fragment of
-blotting or papier Joseph, in order to remove any of the preservative
-solution that may have run from the surface to the underside in the
-previous operation. The plate thus preserved is to be reared on a
-piece of blotting paper with its face against the wall until dry, and
-is then to be stowed away in a plate box, perfectly light-tight to
-await the
-
-[B] A plate, 9 inches by 7, takes about 1 ounce of solution.
-
-
-EXPOSURE IN THE CAMERA.
-
-Collodion plates preserved as above directed, will keep perfectly
-good and sensitive for 12 months at least; and from the appearance of
-the developed image on a plate that has been kept that time, I see
-at present no reason why, if preserved from the damp, they would not
-keep indefinitely. In my experiments, I have never found the least
-difference in sensitiveness, whether the plate be used within a few
-hours of the time of its preparation, or has been kept for months;
-until, however, we have had more experience in the matter, it would
-be safer not to rely on plates more than 12 months old.
-
-The time of exposure in the camera, of course varies in this process,
-under the same circumstances as it does with the wet Collodion; but
-I have found as a general rule, that it is better to give the plate
-a full exposure than to fall into the opposite extreme: that is to
-say, it is preferable to expose the plate sufficient time for the
-deepest shadows to make an impression than to close the dark slide
-at an earlier period, the mode of development allowing considerable
-latitude in this particular. With a 3-inch single lens, 16-inch
-focus, with a ½-inch stop, the usual time for a bright landscape
-will be about 5 minutes; this of course is merely an approximation
-to the time of exposure, the exact time can only be arrived at by
-experience. I do not think I can do better than follow the plan
-adopted in my "Practical Photography," of giving instances of
-under and over exposure, as a means of educating the tyro in the
-appearances that result from these conditions of the plate.
-
-If the exposure has been of too short duration, the image will come
-out under the developing solution with difficulty; and after a
-continued immersion in it will only present the high lights, the deep
-shadows not being represented, or, if so, in so faint a manner as to
-be useless in the picture.
-
-An over exposed plate, when treated with the developing solution,
-will almost immediately give indications of the picture; and in a
-few minutes, the whole of the picture, _deep shadows and all_, will
-come put in unnatural force; on looking through the picture thus
-produced, we shall observe a great flatness in it, there is a want
-of contrast between the various parts, and although by continuing
-the development we might obtain a tolerably intense negative, the
-resulting picture would be flat, meagre, and unsatisfactory: on the
-contrary, a plate that has been exposed for the correct time, will
-comport itself very differently under development from the foregoing.
-
-The sky and high lights will first appear, then the half tones, and
-lastly, the parts of the picture that were in deep shadow will show
-themselves; this effect should take place in about five minutes from
-the time of immersion in the developing bath: a picture that comes
-out sooner than this, is, as a general rule, over exposed; and one
-that is much after the five minutes before it makes its appearance,
-may be considered as under exposed.
-
-We trust that the above instances may be of service in indicating the
-average time required for an exposure of the plate, but we must ask
-the reader not to take the figures given as actual values, but merely
-as very close approximations to the truth. We will imagine the plate
-to have been properly exposed, and proceed to
-
-
-THE DEVELOPMENT OF THE PICTURE.
-
-It is not necessary that the picture should be developed immediately
-after exposure in the camera; any time that is convenient to the
-operator may intervene between the processes, provided the aggregate
-time before and after exposure does not exceed the limits of keeping
-power of the plate.
-
-The development of the picture may be conducted in two ways, either
-by immersing the plate in baths or dishes, or by placing it on the
-levelling stand and treating it with the solutions, in their proper
-order, as detailed below. Each plan possesses certain advantages, but
-it is of little consequence which one is followed. Perhaps there is
-less danger of the film washing off if the plate be treated on the
-levelling stand, and on the other side with large plates it is more
-difficult to cover them evenly with the developing solution than it
-is simply to immerse them in a pan of solution. We say to the reader,
-try both ways, and make your own selection.
-
-The plate upon being removed from the camera is placed face upwards
-in a porcelain or glass dish of a convenient size (not too large),
-and sufficient distilled water is to be poured over it to cover
-the surface thoroughly--this is for the purpose of softening the
-preservative solution, and must be allowed to remain on the plate
-for five minutes; the plate is then to be lifted in and out of the
-water by means of the silver hook. This done, remove the plate to
-a perfectly clean dish, and pour carefully over it the developing
-solution, composed of
-
- Saturated Solution of Gallic Acid (p. 10) 8 ounces.
- Solution of Nitrate of Silver (p. 10) 2 drams.
- THOROUGHLY MIXED.
-
-In a few minutes the picture will begin to make its appearance,
-and will gradually unfold its details under the influence of the
-developer, until the whole of them are apparent; on raising the
-plate, however, when this stage of development is reached, and
-viewing it by transmitted light, the picture will appear weak
-and poor; we must now remove the plate from the bath, and add 2
-drams more of the nitrate silver solution, and having thoroughly
-mixed it with the gallic acid already in the dish, we return the
-partially developed plate, which in the course of a few minutes
-will have acquired a great amount of intensity,--the exact degree
-can be regulated by the time of immersion: when the picture appears
-sufficiently intense, it is to be removed from the developing dish,
-and a gentle stream of water is poured over it, in order to remove
-any adhering developing solution, and stop all further reducing
-action on it.
-
-During the whole time of the development, the gallic acid should
-remain quite clear; it will become slightly discoloured before the
-end of the development, but it ought not at any time to become muddy,
-or it will deposit a sort of sandy sediment on the surface of the
-plate, which cannot be removed by subsequent washing.
-
-The usual time occupied in the development of a successful picture
-is from 20 to 30 minutes, it might be developed much quicker by
-using pyrogallic acid, but at present I give the preference to the
-developer I have described, as I believe it to be more certain, and
-more under the control of the operator than the pyrogallic acid; and
-further, as it is not necessary to watch the development all the time
-it is going on, there can be very little saving of time in the more
-rapid method of bringing out the latent picture.
-
-The picture being washed free from the adhering developing solution,
-is to be placed on the levelling stand, and subjected to the seventh
-part of the process--
-
-
-FIXING THE DEVELOPED IMAGE.
-
-This is accomplished by pouring over the surface of the plate
-sufficient solution of hyposulphite of soda (p. 15) to thoroughly
-cover it, this will dissolve out the unaltered iodide of silver, and
-give us a clear and bright picture, in which the deep shadows should
-be as transparent as the glass itself, and the high lights as dense
-as a piece of metal, the intermediate tones assuming their proper
-positions according to the intensity of the light that was concerned
-in their formation.
-
-When the whole of the yellow iodide of silver is removed, the fixing
-solution may be thrown off, and the plate must be treated with an
-abundance of water; too much cannot well be given at this stage, as
-the hyposulphite adheres with great tenacity to the plate, even
-after a good washing. The back of the plate must be washed as well
-as the front, for I have found that a neglect of this precaution has
-ruined many a fine negative; the hyposulphite remaining at the back
-finding its way by capillary attraction to the surface, and once
-there, its destructive qualities are sure, sooner or later, to render
-themselves evident.
-
-The picture being thoroughly washed, and either dried spontaneously
-or by the fire, has only to be covered with a film of varnish. And
-now comes the last operation, of
-
-
-VARNISHING THE FINISHED NEGATIVE.
-
-Benzoin varnish is the best coating that can be given to a Collodion
-negative. It resists the action of pieces of grit; it does not crack;
-and, above all, it does not, like amber varnish, split off the
-picture on the slightest friction.
-
-The application of this varnish is a very simple matter. The negative
-is to be again placed on a pneumatic plate holder, and the varnish is
-to be poured on to the surface in precisely the same manner as the
-Collodion was at the commencement of the process, the superfluous
-quantity being returned to the bottle: in a few moments the varnish
-will be quite dry and hard, and the plate may be handled with perfect
-safety.
-
-I may mention, as a precaution, in varnishing the plate, that it
-is better to perform that operation in a still atmosphere; as the
-solvent of the gum being chloroform and very volatile, if it were
-conducted in a current of air, there might be some difficulty in
-obtaining an even coating to the picture.
-
-In concluding this description of a process, which is at once simple
-and certain, I would ask the patient attention of those who may do me
-the honor of repeating my experiments. I have endeavoured to render
-the details of the process as intelligible as possible, and if I have
-succeeded in advancing the art of Photography only one step by so
-doing, I consider that it is an ample return for hours and days spent
-in anxious thought and laborious experiment.
-
-
- FINIS.
-
-
- SPECIAL LIST OF REQUISITES
-
- FOR THE
-
- =DRY COLLODION PROCESS,=
-
- SUPPLIED BY
-
- Messrs, BLAND & LONG,
-
- Opticians, & Photographic Instrument Makers
-
- TO THE QUEEN,
-
- =153, FLEET STREET, LONDON.=
-
- * * * * *
-
- BLAND & LONG'S
-
- =IODIZED DRY COLLODION.=
-
-This preparation will keep for an indefinite period, and can be
-exported to any climate, without risk of deterioration.
-
-_Half-pints, 10s.; Pints, 18s._
-
- * * * * *
-
- BLAND & LONG'S
-
- =PRESERVATIVE SOLUTION,=
-
- READY FOR USE.--_1s. per pint._
-
-
- BLAND & LONG'S
-
- =BENZOIN VARNISH,=
-
- FOR PROTECTING THE FINISHED NEGATIVE.
-
- _1s. per oz._
-
-This varnish does not require the plate to be warmed; but dries
-instantly, leaving a perfectly hard transparent coating on the
-picture.
-
- * * * * *
-
- =NITRATE OF SILVER BATH,=
-
- FOR BLAND & LONG'S DRY COLLODION,
-
- Ready for immediate use.--_7s. 6d. per pint._
-
- * * * * *
-
- =PURE CHEMICALS.=
-
- _s._ _d._
-
- Fused Nitrate of Silver, absolutely pure 4 6 per oz.
- Glacial Acetic Acid 1 0 "
- Pure Gelatine 0 6 "
- Pure Citric Acid 0 6 "
- Gallic Acid, pure 1 6 "
- Iodide of Cadmium 3 0 "
- Hyposulphite of Soda 1 0 per lb.
- Pure Sulphuric Æther 0 6 per oz.
- Absolute Alcohol 0 6 "
-
- * * * * *
-
- FOR THE PRICES OF APPARATUS
-
- SEE
-
- =BLAND & LONG'S=
-
- Illustrated Catalogue of Photographic Apparatus
-
- _Sent free by post, on application._
-
-
- SENSITIVE
-
- =DRY COLLODION PLATES,=
-
- READY FOR EXPOSURE IN THE CAMERA.
-
- (=LONG'S PROCESS.=)
-
- * * * * *
-
-Messrs. Bland & Long are now prepared to supply these
-plates, carefully secured in sealed cases, with full directions for
-exposure and development, of all sizes and in any quantity, at the
-following prices:--
-
- Per Doz. | Per Doz.
- s. d. | £. s. d.
- 4¼ × 3¼ 5 0 | 7 × 6 0 14 0
- 5 × 4 6 6 | 8½ × 6½ 0 18 0
- 5½ × 3⅜  6 0 | 9 × 7 1 1 0
- 6¼ × 3⅜  8 6 | 10 × 8 1 6 0
- 6½ × 4¾ 8 6 | 11 × 9 1 13 6
- 6¾ × 3¼ 8 9 | 12 × 10 2 0 0
- 6 × 5 8 6 | 15 × 12 4 0 0
-
-LARGER OR OTHER SIZES TO ORDER.
-
-The advantages of a certain and simple Dry Collodion Process are so
-obvious to those who have practised Photography in the open air, that
-we feel it is merely necessary to introduce the above list to their
-notice with as few remarks as possible.
-
-We would, however, mention a few particulars connected with the
-process for the information of those who have not hitherto practised
-the Dry Collodion process, as detailed by Mr. Long.
-
-The plates as prepared for sale, are hermetically sealed in an
-envelope perfectly impervious to air and moisture, they can therefore
-be exported to any climate without risk of deterioration.
-
-Plates prepared by Mr. Long's process will keep sensitive for almost
-an indefinite period, and can be developed at any time without
-regard to the date of exposure; this, it will be seen, is of immense
-advantage to the tourist, as he can delay the development of the
-whole of his plates until his return.
-
-To those Photographers whose inclinations or want of leisure will not
-admit of their carrying through the first preparation of the plate,
-these Dry Sensitive Plates will be found invaluable, enabling their
-whole energy to be directed to the more careful selection of subject.
-
-The plates being dry, there is no danger of dust settling on their
-surfaces; this point will be appreciated by every Photographer.
-
-The development of the pictures can be conducted in any room whence
-the light can be excluded--as the process is simple and clean--three
-dishes being the only requisites in point of apparatus.
-
-To Officers, Engineers, and Architects, these Dry Plates offer
-a desideratum of no small value, as they are _always ready for
-use_, occupy very little room in travelling, and can be used under
-circumstances which would preclude the adoption of any process that
-had to be carried out on the spot.
-
- * * * * *
-
-
- BLAND & LONG,
-
- Photographic Instrument Makers to the Queen
-
- 153, FLEET STREET, LONDON.
-
-
- THE
-
- =DRY COLLODION PROCESSES.=
-
- * * * * *
-
- Messrs. BLAND & LONG have invented the following
- simple means of
-
- =CHANGING THE DRY COLLODION PLATES=
-
- while working in the fields. The plan has been in use
- for some time, and answers perfectly.
-
- * * * * *
-
- _Price according to size._
-
- _Adapted to Stereoscopic Camera, 15s._
-
- * * * * *
-
-[Illustration]
-
-
-DESCRIPTION AND DIRECTIONS FOR USE.
-
-No matter what process we employ to retain the sensitiveness of our
-plates, it is most objectionable that the glasses should be made to
-slide by their gravity from the plate-box to the slide; for if we
-employ either honey, glycerine, or oxymel as preservative agents, the
-chances are considerably in favor of an amount of dust settling on
-the surface, the dust being in a great part formed by the attrition
-of the roughened edges of the plate against the plate-box. Another
-inconvenience attending the use of a box when the plate has to slide,
-is the danger that exists under that arrangement of ripping the film
-from the edges of the plate by the friction against the groove in the
-box which holds it. These may appear very trivial matters, but they
-are nevertheless great drawbacks to successful operations.
-
-We may mention that the plan we are about to describe is equally
-applicable to all Cameras of moderate size. We will, however, take
-our description from the form of apparatus adapted to a double lens
-Stereoscopic Camera.
-
-The Camera (A) is furnished at its back with two wires (B). On these
-wires slides the plate-box (C), which has previously been fitted at
-its sides with two sockets (D). Just inside the back of the Camera
-box is a spring (E), and on the top of the Camera is a button (F),
-which secures the dark slide in its place.
-
-We now slide the box of prepared plates (C) on to the wires (B), the
-lid of the box opening from the Camera; we then stretch over the
-whole affair, the black light proof covering (G); this completes the
-arrangement, and now for the mode of operating.
-
-The opaque covering is furnished at its side with two elastic rings.
-Into these thrust the hands, so that the rings may firmly encompass
-the wrist. Then open the plate-box, and throw the lid quite back.
-Next unbutton the door of the dark slide, and raise it until the
-spring (E) flies underneath it, and retains it in a horizontal
-position. This we will presume to be done with the right hand; the
-left hand being engaged as soon as the door is opened, in holding
-the plate that is already in the back in its place. The right hand
-being now at liberty, comes to the assistance of the left, and the
-plate that has undergone exposure is safely transferred to the vacant
-groove in the plate-box. This accomplished, the next plate is to
-be placed in the back, and the same operations gone through in the
-inverse order, the left holding the plate in its place, while the
-right releases the door from the influence of the spring (E), and
-re-buttons it, leaving the plate quite safe in the dark slide.
-
-When we require to focus for a fresh picture, it is only necessary
-to remove the dark covering from that part of the Camera where the
-ground glass is placed. The picture can be seen without removing the
-plate-box or the whole of the covering.
-
-It is obvious that there is no limit to the number of glasses that
-can be taken to the field of operations. In this way, several boxes
-holding a dozen each, can be strapped together and placed on the
-Camera, one by one, as occasion or opportunity may direct.
-
- * * * * *
-
- H. Silverlock, Printer, Doctors' Commons.
-
-
- =PRACTICAL PHOTOGRAPHY,=
-
- ON GLASS AND PAPER,
-
- A Manual,
-
- CONTAINING SIMPLE DIRECTIONS FOR THE PRODUCTION OF
-
- =PORTRAITS, VIEWS, &c. BY THE AGENCY OF LIGHT,=
-
- INCLUDING THE
-
- =Collodion, Albumen, Calotype, Waxed Paper, and Positive Paper
- Processes.=
-
- By CHARLES A LONG.
-
- _Fourth Edition, price 1s.; per Post, 1s. 2d._
-
- * * * * *
-
- =ILLUSTRATED PHOTOGRAPHIC CATALOGUE,=
-
- FREE BY POST.
-
- * * * * *
-
- =SPECTACLES:=
-
- WHEN TO WEAR AND HOW TO USE THEM.
-
- ADDRESSED TO
-
- =THOSE WHO VALUE THEIR SIGHT.=
-
- By CHARLES A. LONG,
-
- THIRD EDITION. POST FREE, SIXPENCE.
-
- * * * * *
-
- ALSO,
-
- A DESCRIPTIVE AND GENERAL CATALOGUE
-
- OF
-
- =SCIENTIFIC & EDUCATIONAL INSTRUMENTS=
-
- AND
-
- CHEMICAL PREPARATIONS,
-
- Manufactured and Sold by BLAND & LONG,
-
- =OPTICIANS, PHILOSOPHICAL, PHOTOGRAPHICAL, AND CHEMICAL INSTRUMENT
- MAKERS,=
-
- AND OPERATIVE CHEMISTS.
-
- _Free by Post._
-
- PUBLISHED BY BLAND & LONG, Opticians,
-
- Philosophical and Photographical Instrument Makers
- to the Queen,
-
- 163, FLEET STREET.
-
-
- * * * * *
-
-
-Transcriber Note
-
-Minor typos corrected. Images moved to prevent splitting paragraphs.
-
-
-
-
-
-
-
-End of Project Gutenberg's The Dry Collodion Process, by Charles Long
-
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